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HRID1606423

反应详情

EQUATION

反应方程式

HRID 1606423 的结构方程式

REACTANTS

反应物

3
结构：ClCCl
HCID6344

Dichloromethane

CH2Cl2

结构：CC1(C)S[C@@H]2[C@H](NC(=O)[C@H](N)c3ccccc3)C(=O)N2[C@H]1C(=O)O.O.O.O
HCID23565

Ampicillin Trihydrate

C16H25N3O7S

结构：O=S(=O)([O-])[O-].[Mg+2]
HCID24083

Magnesium sulfate anhydrous

MgO4S

PRODUCTS

生成物

1
结构：CC1(C)S[C@@H]2[C@H](NC(=O)[C@H](N)c3ccccc3)C(=O)N2[C@H]1C(=O)O.CCN(CC)CC
HCID12918994

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

To 14 ml. of dichloromethane were added 806 mg. of ampicillin trihydrate, 600 mg. of magnesium sulfate, and 0.42 ml. of triethylamine and after stirring the mixture for about 1 hour at room temperature, magnesium sulfate was filtered off to provide a dichloromethane solution of ampicillin triethylamine salt.

WORKUP

后处理

  1. filtrationmagnesium sulfate was filtered off