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HRID1606426

反应详情

EQUATION

反应方程式

HRID 1606426 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CC1(C)S[C@@H]2[C@H](NC(=O)[C@H](N)c3ccccc3)C(=O)N2[C@H]1C(=O)O.O.O.O
HCID23565

Ampicillin Trihydrate

C16H25N3O7S

结构：O=S(=O)([O-])[O-].[Mg+2]
HCID24083

Magnesium sulfate anhydrous

MgO4S

PRODUCTS

生成物

1
结构：CC1(C)S[C@@H]2[C@H](NC(=O)[C@H](N)c3ccccc3)C(=O)N2[C@H]1C(=O)O.CCN(CC)CC
HCID12918994

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

After stirring a mixture of 2.0 g. of ampicillin trihydrate, 1.5 g. of magnesium sulfate, 1.05 ml. of triethylamine, and 30 ml. of dichloromethane for 1 hour at room temperature, magnesium sulfate was filtered off to provide a dichloromethane solution of ampicillin triethylamine salt.

WORKUP

后处理

  1. additiona mixture of 2.0 g
  2. filtrationmagnesium sulfate was filtered off