HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 1175-97-9
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ampicillin Trihydrate | HCID 23565 | — |
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1175-97-9 | HCID 12918994 | — |
Reaction Steps
After stirring a mixture of 930 mg. of ampicillin trihydrate, 0.5 ml. of triethylamine, 700 mg. of magnesium sulfate, and 20 ml. of dichloromethane for one hour at room temperature, magnesium sulfate was filtered off to provide a dichloromethane solution of ampicillin triethylamine salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953428 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-09494a144034436cb0db54f08efb7a68 |
| Source note | uspto-grants-1976_04 |