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HRID1606427

反应详情

EQUATION

反应方程式

HRID 1606427 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：CC1(C)S[C@@H]2[C@H](NC(=O)[C@H](N)c3ccccc3)C(=O)N2[C@H]1C(=O)O.O.O.O
HCID23565

Ampicillin Trihydrate

C16H25N3O7S

结构：O=S(=O)([O-])[O-].[Mg+2]
HCID24083

Magnesium sulfate anhydrous

MgO4S

PRODUCTS

生成物

1
结构：CC1(C)S[C@@H]2[C@H](NC(=O)[C@H](N)c3ccccc3)C(=O)N2[C@H]1C(=O)O.CCN(CC)CC
HCID12918994

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

After stirring a mixture of 930 mg. of ampicillin trihydrate, 0.5 ml. of triethylamine, 700 mg. of magnesium sulfate, and 20 ml. of dichloromethane for one hour at room temperature, magnesium sulfate was filtered off to provide a dichloromethane solution of ampicillin triethylamine salt.

WORKUP

后处理

  1. additiona mixture of 930 mg
  2. filtrationmagnesium sulfate was filtered off