HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → 1175-97-9
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Ampicillin Trihydrate | HCID 23565 | — |
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | 1175-97-9 | HCID 12918994 | — |
Reaction Steps
In 60 ml. of dichloromethane was suspended 4.03 g. of ampicillin trihydrate and after adding to the solution 2.1 ml. of triethylamine and 4.0 g. of magnesium sulfate, the mixture was stirred for 30 minutes at room temperature. Then, by filtering off the magnesium sulfate, a dichloromethane solution of ampicillin triethylamine salt was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953428 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-383c4d318b3342039220e76d69e57976 |
| Source note | uspto-grants-1976_04 |