HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → 2,2,6,6-Tetramethyl-4-piperidone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | Acetonin | HCID 68396 | — |
| Product | 2,2,6,6-Tetramethyl-4-piperidone | HCID 13220 | — |
Reaction Steps
17.2 g of acetonine hydrate, 30 g of acetone and 0.5 g of ammonium chloride are heated in a sealed tube for 6 hours at 45° C. After this period of time, it is shown by gas-chromatographical analysis that at least 95% of the employed acetonine has been reacted to form triacetoneamine, which is then isolated by distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953459 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-bc183cf9932a450e895a0ba5592890c9 |
| Source note | uspto-grants-1976_04 |