HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178460115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Propionyl chloride | HCID 62324 | — |
| Reactant | HCID 178509313 | HCID 178509313 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178460115 | HCID 178460115 | — |
Reaction Steps
From 12 g. 3-imino-1-phenyl-3H-1,2-benzisothiazole-1-oxide, 5 g. propionyl chloride and 6.6 g. triethylamine in chloroform, there is obtained, after heating under reflux for 3 hours and then working up the reaction mixture in the usual manner, the desired 3-(propionyl-imino)-1-phenyl-3H-1,2-benzisothiazole-1-oxide which, after recrystallisation from ethyl acetate, melts at 170°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953464 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-6f0d2aeb73354c8e9a625681576aeaa5 |
| Source note | uspto-grants-1976_04 |