HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetyl chloride → HCID 178520253, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetyl chloride | HCID 7679 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 178509313 | HCID 178509313 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178520253 | HCID 178520253 | — |
Reaction Steps
2.4 g. 3-imino-1-phenyl-3H-1,2-benzisothiazole-1-oxide are boiled for 1 hour with 1.32 g. triethylamine and 1.6 g. phenylacetyl chloride in 50 cc. chloroform. After working up in the usual manner, there is obtained 3-(phenylacetylimino)-1-phenyl-3H-1,2-benzisothiazole-1-oxide in the form of yellow crystals which, after recrystallisation from ethyl acetate, melt at 120°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953464 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-6ea3e0e8ac6d4cb8b12e82cb088e3196 |
| Source note | uspto-grants-1976_04 |