HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 21544131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21544128 | HCID 21544128 | — |
| Solvent | Dimethylacetamide | HCID 31374 | — |
| Product | HCID 21544131 | HCID 21544131 | — |
Reaction Steps
A solution of 2,4,6-triiodo-5-methoxyacetamido-N-methylisophthalamic acid in N,N-dimethylacetamide is treated with an excess of thionyl chloride. After the reaction, the excess thionyl chloride is removed by evaporation and the product is suitable for use as intermediate in situ.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953497 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-4f7bf19807f5496998875539a67e61d3 |
| Source note | uspto-grants-1976_04 |