HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 21427248, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Dimethylacetamide | HCID 31374 | — |
| Reactant | HCID 21427255 | HCID 21427255 | — |
| Product | HCID 21427248 | HCID 21427248 | — |
Reaction Steps
Analogously to Example 3, 71.5 g. (74.5%) of N-3-carboxy-5-acetamido-2,4,6-triiodobenzoyl)-sarcosine methylamide, m.p. 270°-271° C. (under decomposition) is obtained from 90 g. (0.14 mole) of N-(3-carboxy-5-amino-2,4,6-triiodobenzoyl)-sarcosine methylamide (IV e), m.p. 238°-240° C. (decomposition) in 170 ml. of dimethylacetamide and 27.4 ml. of acetyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953501 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-3947b44e9815438f9f9080261a88118c |
| Source note | uspto-grants-1976_04 |