Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 1,2,3,4-Tetrahydro-1-naphthylamine | HCID 18066 | — |
| Reactant | (+)-N-Benzoylglutamic acid | HCID 11207465 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 70616871 | HCID 70616871 | — |
Reaction Steps
A stirred mixture of 284 grams (1.13 moles) of (R)-(+)-N-benzoylglutamic acid, 136 grams (2.26 moles) of acetic acid, and 2 liters of water is heated to 55° C. to give a solution. To this stirred solution is added 333 grams (2.26 moles) of racemic 1,2,3,4-tetrahydro-1-naphthylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US03953506 |
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| Source dataset | uspto-grants-1976_04 |
|---|
| ORD ID | ord-adf8a74f07714f5cb1805267e9abaa74 |
|---|
| Source note | uspto-grants-1976_04 |
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