HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 21544473, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 3-Chloro-5-mercaptobenzoic acid | HCID 21542330 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21544473 | HCID 21544473 | 70% |
Reaction Steps
In a manner similar to procedure of Example 14, 3-mercapto-5-chlorobenzoic acid is contacted with methyl iodide in methanol containing potassium hydroxide as the base to yield the desired product in 70% yield, m.p. 148°-150° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953595 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-386271569b4e45ca9dd785fe67619564 |
| Source note | uspto-grants-1976_04 |