HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 3-Methoxy-5-(trifluoromethyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 3-hydroxy-5-(trifluoromethyl)benzoic Acid | HCID 2783146 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Methoxy-5-(trifluoromethyl)benzoic acid | HCID 21544467 | — |
Reaction Steps
This product is prepared according to the procedure of Example 5 and comprises contacting 3-hydroxy-5-trifluoromethylbenzoic acid with methyl iodide in methanol containing sodium methoxide as the base, m.p. 131°-135° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953595 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-b92fa04e02ba4fd087351bc967c99679 |
| Source note | uspto-grants-1976_04 |