HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nicotinic Acid → 3-Pyridinecarbonyl chloride, hydrochloride (1:1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nicotinic Acid | HCID 938 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 3-Pyridinecarbonyl chloride, hydrochloride (1:1) | HCID 88438 | — |
Reaction Steps
A mixture of 90 grams of nicotinic acid and 180 ml of thionyl chloride were heated at 55°-65° C. for 3.5 hours. The excess thionyl chloride was removed in vacuum and nicotinoyl chloride-hydrochloride was obtained
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03953596 |
| Source dataset | uspto-grants-1976_04 |
| ORD ID | ord-5df2b4ef3cbd4979a0997afef0064690 |
| Source note | uspto-grants-1976_04 |