Hexadecylamine → HCID 86743343, compound

HRID 1606869Notes

Reaction equation

HRID 1606869 reaction equation
[CH2:1]([NH2:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[CH2:18]1[O:20][CH:19]1[CH2:21][OH:22]>>[CH2:1]([NH2:17])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH3:16].[CH2:18]1[O:20][CH:19]1[CH2:21][OH:22]

Participants

3

Reactant 2

HCID 8926Hexadecylamine3×HCID 11164Glycidol2×

Product 1

HCID 86743343HCID 86743343, compound

Procedure

Into a reactor fitted with a dropping funnel, a N2 gas inlet, a stirrer, a thermometer, a condenser, and a gas vent, was placed 36 g (0.15 mole) of hexadecylamine. Under a nitrogen atmosphere, glycidol (55.5 g, 0.75 mole) was added dropwise to the hexadecylamine at 150° to 160° C. Upon completion of the addition, the reaction mixture was stirred at 150° to 160° C. for an additional 45 minutes. The reaction mixture was cooled and the product removed from the flask. The product, identified as a hexadecylamine adduct with 5 moles of glycidol, weighed 91 grams.

Workup

  1. customInto a reactor fitted with a dropping funnel, a N2 gas inlet, a stirrer
  2. additionUpon completion of the addition
  3. temperatureThe reaction mixture was cooled
  4. customthe product removed from the flask

Sources & evidence

ORD record
ord-35d3657c71e046baaf1184fa41a23d62
Source dataset
uspto-grants-1989_09
Patent number
US04863563

Reaction notes

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