Chlorosuccinimide → HCID 131716091, compound

HRID 1607071Notes

Reaction equation

HRID 1607071 reaction equation
[Cl:1]N1C(=O)CCC1=O.Br[C:10]1[CH:11]=[C:12]2[C:25]3[C:15]([CH2:16][C@@H:17]4[C@@H:22]([C:23]=3[CH:24]=1)[CH2:21][C@H:20]([NH:26][C:27](=[O:33])[N:28]([CH2:31][CH3:32])[CH2:29][CH3:30])[CH2:19][N:18]4[CH3:34])=[CH:14][N:13]2[Si](C(C)(C)C)(C)C>>[Cl:1][C:24]1[C:23]2=[C:25]3[C:12]([NH:13][CH:14]=[C:15]3[CH2:16][C@@H:17]3[C@@H:22]2[CH2:21][C@H:20]([NH:26][C:27](=[O:33])[N:28]([CH2:31][CH3:32])[CH2:29][CH3:30])[CH2:19][N:18]3[CH3:34])=[CH:11][CH:10]=1

Participants

3

Reactant 2

HCID 31398ChlorosuccinimideHCID 13823172HCID 13823172, compound

Product 1

HCID 131716091HCID 131716091, compound

Procedure

With N-chlorosuccinimide and 3-(13-bromo-1-tert-butyldimethylsilyl-6-methyl-8α-ergolinyl)-1 1-diethylurea:

Sources & evidence

ORD record
ord-d4aac752e44c4ed6af08b39ce794e225
Source dataset
uspto-grants-1989_09
Patent number
US04863929

Reaction notes

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