Chlorosuccinimide → HCID 131716092, compound

HRID 1607072Notes

Reaction equation

[Cl:1]N1C(=O)CCC1=O.Br[C:10]1[CH:11]=[C:12]2[C:25]3[CH:15]([CH2:16][C@@H:17]4[C@@H:22]([C:23]=3[CH:24]=1)[CH2:21][C@H:20]([NH:26][C:27](=[O:33])[N:28]([CH2:31][CH3:32])[CH2:29][CH3:30])[CH2:19][N:18]4[CH3:34])[CH2:14][N:13]2[Si](C(C)(C)C)(C)C>>[Cl:1][C:10]1[CH:11]=[C:12]2[C:25]3[C:15]([CH2:16][C@@H:17]4[C@@H:22]([C:23]=3[CH:24]=1)[CH2:21][C@H:20]([NH:26][C:27](=[O:33])[N:28]([CH2:31][CH3:32])[CH2:29][CH3:30])[CH2:19][N:18]4[CH3:34])=[CH:14][NH:13]2

Participants

Reactant 2

HCID 31398Chlorosuccinimide

HCID 131716087HCID 131716087, compound

Product 1

HCID 131716092HCID 131716092, compound

Procedure

With N-chlorosuccinimide and 3-(13-bromo-1-tert-butyldimethylsilyl-2,3-dihydro-6-methyl-8α-ergolinyl)-1,1-diethylurea:

Sources & evidence

ORD record: ord-3e8c13a2976b453595cfc853bbc679aa
Source dataset: uspto-grants-1989_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04863929

Reaction notes

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