Chlorosuccinimide → HCID 131716093, compound

HRID 1607073Notes

Reaction equation

HRID 1607073 reaction equation
[Cl:1]N1C(=O)CCC1=O.Br[C:10]1[C:24]2=[C:25]3[C:13]([N:14]([Si](C(C)(C)C)(C)C)[CH:15]=[C:16]3[CH2:17][C@@H:18]3[C:23]2=[CH:22][C@H:21]([NH:26][C:27](=[O:33])[N:28]([CH2:31][CH3:32])[CH2:29][CH3:30])[CH2:20][N:19]3[CH3:34])=[CH:12][CH:11]=1>>[Cl:1][C:11]1[CH:12]=[C:13]2[C:25]3[CH:16]([CH2:17][C@@H:18]4[C@@H:23]([C:24]=3[CH:10]=1)[CH2:22][C@H:21]([NH:26][C:27](=[O:33])[N:28]([CH2:31][CH3:32])[CH2:29][CH3:30])[CH2:20][N:19]4[CH3:34])[CH2:15][NH:14]2

Participants

3

Reactant 2

HCID 31398ChlorosuccinimideHCID 131716094HCID 131716094, compound

Product 1

HCID 131716093HCID 131716093, compound

Procedure

With N-chlorosuccinimide and 3-(12-bromo-1-tert-butyldimethylsilyl-9,10-didehydro-6-methyl-8α-ergolinyl)1,1-diethylurea:

Sources & evidence

ORD record
ord-8a9b5093389c48cbb0ffc14203cc3b2b
Source dataset
uspto-grants-1989_09
Patent number
US04863929

Reaction notes

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