Hydrochloric Acid → HCID 19838480, compound

HRID 1607136Notes

Reaction equation

HRID 1607136 reaction equation
Cl.O.[O:3]1[CH2:7][CH2:6][C:5]2[CH:8]=[C:9]3[C:14](=[CH:15][C:4]1=2)[C:13](=O)[CH2:12][CH2:11][CH2:10]3>[Zn].C1(C)C=CC=CC=1>[O:3]1[CH2:7][CH2:6][C:5]2[CH:8]=[C:9]3[C:14](=[CH:15][C:4]1=2)[CH2:13][CH2:12][CH2:11][CH2:10]3

Participants

6

Reactant 3

HCID 313Hydrochloric AcidHCID 962WaterHCID 14234809HCID 14234809, compound

Product 1

HCID 19838480HCID 19838480, compound

Reagents, catalysts & solvents 2

HCID 23994ZincCatalystHCID 1140TolueneSolvent

Procedure

An amalgam of zinc and mercuric chloride (72 g Zn and 7.1 g HgCl2) is added to a mixture containing 120 ml of concentrated hydrochloric acid, 57 ml of water, 30 g of the compound of Example 1 and 71 ml of toluene, with stirring.

Sources & evidence

ORD record
ord-4bdfaf3c0a4541cb800977fa5d342865
Source dataset
uspto-grants-1989_09
Patent number
US04863951

Reaction notes

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