HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3-Bromopropoxy)-3-nitrobenzene → 3-(3-Bromopropoxy)-aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3-Bromopropoxy)-3-nitrobenzene | HCID 7172301 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 3-(3-Bromopropoxy)-aniline | HCID 459256 | — |
Reaction Steps
1 g of Raney nickel is added to a solution of 4 g of 3-(3-bromopropoxy)-nitrobenzene in 40 ml of tetrahydrofuran and the whole is hydrogenated at room temperature. The catalyst is filtered off and washed with tetrahydrofuran. After concentration of the filtrate by evaporation, 3-(3-bromopropoxy)-aniline is obtained in the form of a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04863942 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-043d700601ea430599564253e865b5dd |
| Source note | uspto-grants-1989_09 |