HRID1607162
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
1 g of Raney nickel is added to a solution of 4 g of 3-(3-bromopropoxy)-nitrobenzene in 40 ml of tetrahydrofuran and the whole is hydrogenated at room temperature. The catalyst is filtered off and washed with tetrahydrofuran. After concentration of the filtrate by evaporation, 3-(3-bromopropoxy)-aniline is obtained in the form of a colourless oil.
WORKUP
后处理
- customis hydrogenated at room temperature
- filtrationThe catalyst is filtered off
- washwashed with tetrahydrofuran
- customAfter concentration of the filtrate by evaporation