HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14579773, compound → HCID 14579774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14579773 | HCID 14579773 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14579774 | HCID 14579774 | — |
Reaction Steps
A solution of 2-(p-methoxyphenethyl)-3-methyl-4-hydroxy-5-allylbenzofuran (0.65 gm, 2 mmoles) in ethanol (50 mL) was hydrogenated in a Parr hydrogenator in the presence of 5% palladium on charcoal at 50 psi for a period of 2 hours. The catalyst was filtered off and the filtrate was concentrated in vacuo to yield 2-(p-methoxyphenethyl)-3-methyl-4-hydroxy-5-propylbenzofuran, mp 77°-79° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04863958 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-56da9e83620f4e0b8b95668cc85ad49a |
| Source note | uspto-grants-1989_09 |