HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 14570909, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Hexamethylenetetramine | HCID 4101 | — |
| Reactant | 4-chloro-6-propylbenzene-1,3-diol | HCID 238173 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 14570909 | HCID 14570909 | — |
Reaction Steps
To a solution of 2-chloro-4-propyl-1,5-dihydroxybenzene (from Step a, 243 mg, 1.3 mmol) in 10 mL trifluoroacetic acid was added 1 g of hexamine. The mixture was refluxed for 20 h. Water was added and the mixture was extracted with ethyl acetate. Chromatography of the concentrated organic extracts gave the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04863958 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-5313288abca543b3812b35780c5d7e4a |
| Source note | uspto-grants-1989_09 |