HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ozone → HCID 13933696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ozone | HCID 24823 | — |
| Reactant | HCID 13933695 | HCID 13933695 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 13933696 | HCID 13933696 | 89% |
Reaction Steps
Ozone gas was bubbled at -78° C. into a solution of 3.48 g (10.0 mmol) of pentafluorophenylmethyl 2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate obtained in Reference Example 4, in 20 ml of ethyl acetate. The subsequent operation was conducted in the same manner as in Reference Example 5, whereby 2.87 g of pentafluorophenylmethyl 2,2-dimethyl-3-formylcyclopropanecarboxylate was obtained as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04864052 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-2458a32ff73e44b1827b5ba7e2aaa925 |
| Source note | uspto-grants-1989_09 |