Acryloyl chloride → HCID 19376127, compound

HRID 1607377Notes

Reaction equation

HRID 1607377 reaction equation
[CH2:1]([O:3][CH:4]([O:10][CH2:11][CH3:12])[CH:5]([NH2:9])[CH2:6][CH2:7][CH3:8])[CH3:2].[C:13](Cl)(=[O:16])[CH:14]=[CH2:15]>C(Cl)Cl>[CH2:11]([O:10][CH:4]([O:3][CH2:1][CH3:2])[CH:5]([NH:9][C:13](=[O:16])[CH:14]=[CH2:15])[CH2:6][CH2:7][CH3:8])[CH3:12]

Participants

4

Reactant 2

HCID 13140Acryloyl chlorideHCID 79006390HCID 79006390, compound

Product 1

HCID 19376127HCID 19376127, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

This compound was made from 25 g (0.14 mol) of aminopentanal diethyl acetal, 12.9 g of acryloyl chloride, 35 g of 14N NaOH and 65 mL of CH2Cl2 using the same procedures as for ABDA (no pH adjustment). The product (32.5 g) had a gc retention time of 7.80 min.

Sources & evidence

ORD record
ord-21d7398e36f04874ad17e71b3c5e8ef6
Source dataset
uspto-grants-1989_09
Patent number
US04864055

Reaction notes

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