HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acryloyl chloride → HCID 19376127, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | HCID 79006390 | HCID 79006390 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19376127 | HCID 19376127 | — |
Reaction Steps
This compound was made from 25 g (0.14 mol) of aminopentanal diethyl acetal, 12.9 g of acryloyl chloride, 35 g of 14N NaOH and 65 mL of CH2Cl2 using the same procedures as for ABDA (no pH adjustment). The product (32.5 g) had a gc retention time of 7.80 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04864055 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-21d7398e36f04874ad17e71b3c5e8ef6 |
| Source note | uspto-grants-1989_09 |