HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 348326, compound → HCID 12308369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 348326 | HCID 348326 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 12308369 | HCID 12308369 | 99.2% |
Reaction Steps
A solution of 13.6 g of the ester compound obtained in 300 ml of benzene was hydrogenated over 1.3 g of a 10% palladium/charcoal under atmospheric pressure. After filtration of the catalyst, the filtrate was concentrated under reduced pressure to obtain 13.6 g of 2-cyano-3-(1-naphthyl)propionic acid ethyl ester as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04863904 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-12c5fd5e0a2745a4a322e1206979e939 |
| Source note | uspto-grants-1989_09 |