HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 19850512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 19850511 | HCID 19850511 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19850512 | HCID 19850512 | — |
Reaction Steps
A suspension of 50 g of hydrogen-reduced iron powder in 150 ml of ethanol, to which 7 ml of water and 5 ml of acetic acid have been added, is heated under reflux. 0.08 mole (20.3 g) of 5-methoxy-6-nitro-2-methyl-2-propyl-1,3-benzodioxole is added portionwise. Heating is continued for 30 minutes after the end of the addition. The reaction mixture is filtered while boiling. 25 ml of a 7N solution of hydrochloric acid is added to the filtrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04865617 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-37c0e9c54d4e49ec929931bb04a01d62 |
| Source note | uspto-grants-1989_09 |