HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumarate → 5-Methyl-2-(1-methyl-1,2,5,6-tetrahydro-3-pyridyl)-thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumarate | HCID 5460307 | — |
| Reactant | 5-Methyl-2-(3-pyridyl)-thiazole | HCID 19612513 | — |
| Product | 5-Methyl-2-(1-methyl-1,2,5,6-tetrahydro-3-pyridyl)-thiazole | HCID 19612479 | — |
Reaction Steps
The title compound was prepared from 88 (2.2 g, 0.013 mol) by the procedure described in Example 49. The crude free base obtained, 89, was converted to the title fumarate, 90. Yield: 0.8 g (0.0032 mol, 25%). M.P. 159°-160° C. Anal. (C12H16N2O2S)C, H, N.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04866077 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-20be5756eb964adc8d62a76ecbb0ba26 |
| Source note | uspto-grants-1989_09 |