HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus pentachloride → HCID 10448313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus pentachloride | HCID 24819 | — |
| Reactant | HCID 10402218 | HCID 10402218 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 10448313 | HCID 10448313 | 103.5% |
Reaction Steps
A mixture of 3-(2,4-difluorophenoxy)-4-nitrobenzoic acid (1 g) and phosphorus pentachloride (0.74 g) in benzene (10 ml) was stirred for 30 minutes at room temperature. Benzene was evaporated under reduced pressure to give an oil of 3-(2,4-difluorophenoxy)-4-nitrobenzoyl chloride (1.1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04866091 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-640483cf46be44968e71f30b77f34dec |
| Source note | uspto-grants-1989_09 |