Hydrochloric Acid → HCID 11726065, compound

Participants

Reaction Steps

A mixture of 2-methyl-2-[4-nitro-3-(2,4,6-trichlorophenoxy)phenyl]-1,3-dioxolane (1.7 g) and 3N-hydrochloric acid (5 ml) in acetone (15 ml) was refluxed for 2 hours. The mixture was concentrated under reduced pressure. To the residue were added water and ethyl acetate. The organic layer was dried and concentrated to give a powder of 4'-nitro-3'-(2,4,6-trichlorophenoxy)acetophenone (1.5 g).

Provenance & Evidence