Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | HCID 131716109 | HCID 131716109 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 10000027 | HCID 10000027 | — |
Reaction Steps
To a stirred solution of 4'-acetyl-2'-(2-methylthiophenoxy)methanesulfonanilide (1.2 g) in acetic acid (7 ml) was added dropwise 30% hydrogen peroxide (1 ml). The mixture was stirred for 2 hours at 70° C. and cooled to room temperature. Ethanol (10 ml) was added, and the precipitates were filtered and washed with ethanol to give colorless needles of 4'-acetyl-2'-(2-methylsulfonylphenoxy)methanesulfonanilide (1.1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04866091 |
|---|
| Source dataset | uspto-grants-1989_09 |
|---|
| ORD ID | ord-5a8379ecc8814721aaadbb330e405dba |
|---|
| Source note | uspto-grants-1989_09 |
|---|
