HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2-Dimethoxyethylmethylamine → N-(2,2-Dimethoxyethyl)-N,2-dimethylprop-2-enamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2-Dimethoxyethylmethylamine | HCID 8503 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-(2,2-Dimethoxyethyl)-N,2-dimethylprop-2-enamide | HCID 15332976 | — |
Reaction Steps
Using the above procedure, a methacrylamide monomer was prepared from 23.23 g methacryloyl chloride, 24.53 g N-methylaminoacetaldehyde dimethyl acetal, 42 g NaOH (20% aqueous solution), and 90 ml methylene chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04866151 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-ed6ad41f15fb41c3932c45ddfafec650 |
| Source note | uspto-grants-1989_09 |