2,2-Dimethoxyethylmethylamine → N-(2,2-Dimethoxyethyl)-N,2-dimethylprop-2-enamide

HRID 1607702Notes

Reaction equation

HRID 1607702 reaction equation
[C:1](Cl)(=[O:5])[C:2]([CH3:4])=[CH2:3].[CH3:7][O:8][CH:9]([O:13][CH3:14])[CH2:10][NH:11][CH3:12].[OH-].[Na+]>C(Cl)Cl>[CH3:7][O:8][CH:9]([O:13][CH3:14])[CH2:10][N:11]([CH3:12])[C:1](=[O:5])[C:2]([CH3:4])=[CH2:3]

Participants

5

Reactant 3

HCID 85032,2-DimethoxyethylmethylamineHCID 13528Methacryloyl chlorideHCID 14798Sodium Hydroxide

Product 1

HCID 15332976N-(2,2-Dimethoxyethyl)-N,2-dimethylprop-2-enamide

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Using the above procedure, a methacrylamide monomer was prepared from 23.23 g methacryloyl chloride, 24.53 g N-methylaminoacetaldehyde dimethyl acetal, 42 g NaOH (20% aqueous solution), and 90 ml methylene chloride.

Sources & evidence

ORD record
ord-ed6ad41f15fb41c3932c45ddfafec650
Source dataset
uspto-grants-1989_09
Patent number
US04866151

Reaction notes

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