HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19785757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methacryloyl chloride | HCID 13528 | — |
| Reactant | HCID 13382128 | HCID 13382128 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19785757 | HCID 19785757 | — |
Reaction Steps
Following the above procedure, the monomer was prepared using 22 g triethylamine, 35.2 g 2-[2-(2-hydroxyethoxy)-propyl]-1,3-dioxolane, 23.22 g methacryloyl chloride, and 180 ml methylene chloride. The product was purified by vacuum distillation at 93.2° C. under 0.2 mm Hg pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04866151 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-1b522536235c484f8b7ed3174a82c333 |
| Source note | uspto-grants-1989_09 |