Triethylamine → HCID 19785757, compound

HRID 1607705Notes

Reaction equation

HRID 1607705 reaction equation
C(N(CC)CC)C.[OH:8][CH2:9][CH2:10][O:11][CH:12]([CH3:19])[CH2:13][CH:14]1[O:18][CH2:17][CH2:16][O:15]1.[C:20](Cl)(=[O:24])[C:21]([CH3:23])=[CH2:22]>C(Cl)Cl>[C:20]([O:8][CH2:9][CH2:10][O:11][CH:12]([CH3:19])[CH2:13][CH:14]1[O:15][CH2:16][CH2:17][O:18]1)(=[O:24])[C:21]([CH3:23])=[CH2:22]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 13528Methacryloyl chlorideHCID 13382128HCID 13382128, compound

Product 1

HCID 19785757HCID 19785757, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Following the above procedure, the monomer was prepared using 22 g triethylamine, 35.2 g 2-[2-(2-hydroxyethoxy)-propyl]-1,3-dioxolane, 23.22 g methacryloyl chloride, and 180 ml methylene chloride. The product was purified by vacuum distillation at 93.2° C. under 0.2 mm Hg pressure.

Workup

  1. customthe monomer was prepared
  2. distillationThe product was purified by vacuum distillation at 93.2° C. under 0.2 mm Hg pressure

Sources & evidence

ORD record
ord-1b522536235c484f8b7ed3174a82c333
Source dataset
uspto-grants-1989_09
Patent number
US04866151

Reaction notes

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