HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetaldehyde → Quindoxin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetaldehyde | HCID 177 | — |
| Reactant | Benzofuroxan | HCID 68075 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | Quindoxin | HCID 72073 | — |
Reaction Steps
A mixture of benzofuroxan (2.5 g.), acetaldehyde (2.5 ml.) and triethylamine (20 ml.) is allowed to stand at room temperature for 24 hours. The solid material which precipitates is filtered and dried to give product, M.P. 223°-224° C. dec. (MIC against P. vulgaris is 12.5 mcg./ml.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04866175 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-8ce7d3dd4f95463ab3b62df2f02df71b |
| Source note | uspto-grants-1989_09 |