HRID1607718

反应详情

EQUATION

反应方程式

HRID 1607718 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of benzofuroxan (2.5 g.), acetaldehyde (2.5 ml.) and triethylamine (20 ml.) is allowed to stand at room temperature for 24 hours. The solid material which precipitates is filtered and dried to give product, M.P. 223°-224° C. dec. (MIC against P. vulgaris is 12.5 mcg./ml.).

WORKUP

后处理

  1. customThe solid material which precipitates
  2. filtrationis filtered
  3. customdried
  4. customto give product, M.P. 223°-224° C. dec. (MIC against P. vulgaris is 12.5 mcg./ml.)