HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitropropane → HCID 178430959, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitropropane | HCID 398 | — |
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | Benzofuroxan | HCID 68075 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178430959 | HCID 178430959 | — |
Reaction Steps
To a mixture containing 2-nitropropane (10.7 g., 0.12 moles), benzofuroxan (13.6 g., 0.10 moles) and tetrahydrofuran (50 ml.) is added dropwise diethylamine (8.7 g., 0.12 mole). The reaction temperature rises during addition. Upon completion of addition, the reaction mixture is allowed to sit overnight at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04866175 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-785d365accf046d6b37486f249bd7529 |
| Source note | uspto-grants-1989_09 |