Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 2,5-Dichlorobenzenesulfonyl chloride | HCID 79401 | — |
| Reactant | HCID 14579442 | HCID 14579442 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14579447 | HCID 14579447 | — |
Reaction Steps
A mixture of 2.95 g of (±)-4-(2-amino-1-methylethyl)phenoxyacetic acid hydrochloride, 3.82 g of sodium carbonate, 30 ml of water and 3.1 g of 2,5-dichlorophenylsulfonyl chloride is stirred at 80° C. for 3 hours. The reaction mixture is treated in the same manner as described in Example 43, whereby (±)-4-[2-(2,5-dichlorophenyl)sulfonylamino-1-methylethyl)phenoxyacetic acid is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04866196 |
|---|
| Source dataset | uspto-grants-1989_09 |
|---|
| ORD ID | ord-54a0daa4f87e49d2a9997135a8cd7bc1 |
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| Source note | uspto-grants-1989_09 |
|---|
