P-Toluic Acid → HCID 54121849, compound

HRID 1607773Notes

Reaction equation

HRID 1607773 reaction equation
CC(CCCCC)CCCCC1C=CC(C(O)=O)=CC=1.[CH2:21]([O:29][C:30]1[CH:35]=[CH:34][C:33](O)=[CH:32][CH:31]=1)[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26]CC.[CH3:37][CH:38]([CH2:54][CH2:55][CH2:56][CH3:57])[CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44][C:45]1[CH:53]=[CH:52][C:48]([C:49]([OH:51])=[O:50])=[CH:47][CH:46]=1.CC(CCCC)CCCCCBr.CC1C=CC(C(O)=O)=CC=1.C(OC1C=CC(O)=CC=1)CCCCC>>[CH2:21]([O:29][C:30]1[CH:31]=[CH:32][C:33]([O:50][C:49](=[O:51])[C:48]2[CH:47]=[CH:46][C:45]([CH2:44][CH2:43][CH2:42][CH2:41][CH2:40][CH2:39][CH:38]([CH3:37])[CH2:54][CH2:55][CH2:56][CH3:57])=[CH:53][CH:52]=2)=[CH:34][CH:35]=1)[CH2:22][CH2:23][CH2:24][CH2:25][CH3:26]

Participants

7

Reactant 6

HCID 7470P-Toluic AcidHCID 293544-HexyloxyphenolHCID 77412Phenol, 4-(octyloxy)-HCID 14496338HCID 14496338, compoundHCID 19851074HCID 19851074, compoundHCID 198510754-(5'-Methyldecyl)benzoic acid

Product 1

HCID 54121849HCID 54121849, compound

Procedure

The procedure of Example 1 was followed except that the 4-(5'-methyldecyl)benzoic acid and 4-n-octoxyphenol were replaced by 4-(7'-methylundecyl)benzoic acid prepared by reacting 6-methyldecylbromide with 4-methylbenzic acid and 4-n-hexyloxyphenol to thereby give the title compound.

Workup

  1. customprepared

Sources & evidence

ORD record
ord-ec00fe407ab840fda28dcafb3064221b
Source dataset
uspto-grants-1989_09
Patent number
US04866199

Reaction notes

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