Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Diethanolamine | HCID 8113 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Fluoro-4'-nitro-1,1'-biphenyl | HCID 96413 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 19849273 | HCID 19849273 | — |
Reaction Steps
A one liter three necked flask fitted with a mechanical stirrer, condenser and thermometer is charged with 21.7 g of 4-fluoro-4'-nitrobiphenyl, 31.0 g of diethanolamine, 13.8 g of potassium carbonate, 1.0 g of Aliquot 336, and 500 ml of dimethyl sulfoxide. The reaction mixture is heated at 95° C. for a period of three days, cooled, and poured into 4 litersof ice water. The crude solid product is filtered, washed with water, and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04867540 |
|---|
| Source dataset | uspto-grants-1989_09 |
|---|
| ORD ID | ord-7e7daac6a8df4634a840c3a3164833e4 |
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| Source note | uspto-grants-1989_09 |
|---|
