HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 284115, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Reactant | alpha-Hydroxyacetophenone | HCID 68490 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 284115 | HCID 284115 | — |
Reaction Steps
A mixture of 3.8 g (0.028 mole) of 2-hydroxyacetophenone, 30 g of potassiumhydroxide dissolved in 15 ml of water and 50 ml of ethanol, and 3.8 g (0.028 mole) of anisaldehyde is stirred at ambient temperature for 1 and ahalf hours. The mixture is then poured into a 10% solution of hydrochloric acid. The precipitate formed is filtered off, washed with water and dried.It is recrystallized from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04867964 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-3e4c8b4a6cdf41b28eb6a450aade29ed |
| Source note | uspto-grants-1989_09 |