Hydrochloric Acid → HCID 284115, compound

HRID 1607800Notes

Reaction equation

HRID 1607800 reaction equation
O[CH2:2][C:3]([C:5]1[CH:10]=[CH:9][CH:8]=[CH:7][CH:6]=1)=O.[OH-:11].[K+].[CH3:13][O:14][C:15]1[CH:16]=[CH:17][C:18]([CH:21]=[O:22])=[CH:19][CH:20]=1.Cl>O.C(O)C>[OH:11][C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=1[CH:3]=[CH:2][C:21]([C:18]1[CH:19]=[CH:20][C:15]([O:14][CH3:13])=[CH:16][CH:17]=1)=[O:22]

Participants

7

Reactant 4

HCID 313Hydrochloric AcidHCID 14797Potassium HydroxideHCID 312444-MethoxybenzaldehydeHCID 68490alpha-Hydroxyacetophenone

Product 1

HCID 284115HCID 284115, compound

Reagents, catalysts & solvents 2

HCID 702EthanolSolventHCID 962WaterSolvent

Procedure

A mixture of 3.8 g (0.028 mole) of 2-hydroxyacetophenone, 30 g of potassiumhydroxide dissolved in 15 ml of water and 50 ml of ethanol, and 3.8 g (0.028 mole) of anisaldehyde is stirred at ambient temperature for 1 and ahalf hours. The mixture is then poured into a 10% solution of hydrochloric acid. The precipitate formed is filtered off, washed with water and dried.It is recrystallized from ethanol.

Workup

  1. customThe precipitate formed
  2. filtrationis filtered off
  3. washwashed with water and dried.It
  4. customis recrystallized from ethanol

Sources & evidence

ORD record
ord-3e4c8b4a6cdf41b28eb6a450aade29ed
Source dataset
uspto-grants-1989_09
Patent number
US04867964

Reaction notes

Loading…