1-Dodecanethiol → HCID 21613593, compound

Participants

Reaction Steps

36 g of dodecane thiol are converted into the corresponding sulphenic acid chloride by reaction with sulphuryl chloride as described above. This compound is added to a suspension of 56 g of the compound obtainable under (a). The mixture is then stirred for 2 hours and concentrated by evaporation and the residue is recrystallized from ethanol. m.p. 56° to 57° C.

Provenance & Evidence