HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → HCID 14181181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Methyl chloroacetate | HCID 7295 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 6-Hydroxy-3,4-dihydro-1(2H)-naphthalenone | HCID 4679494 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 14181181 | HCID 14181181 | — |
Reaction Steps
1 mol of 6-hydroxy-1-tetralone, 1.2 mols of methyl chloroacetate, 2 mols of potassium carbonate and 0.1 mol of potassium iodide are boiled under reflux in 2 1 of butanone for 6 hours. The mixture is filtered, the residue is rinsed with acetone and the filtrate is evaporated. The residue is taken up in methylene chloride, and the mixture is washed 3 times with 0.5 N NaOH solution, dried over sodium sulphate and evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04868332 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-9d184557256242c9b3bd38778260260c |
| Source note | uspto-grants-1989_09 |