HCID 14014974, compound → HCID 14014982, compound

HRID 1608060Notes

Reaction equation

HRID 1608060 reaction equation
C([NH:4][CH:5]1[CH2:14][CH2:13][C:12]2[C:11]([O:15][CH2:16][C:17]([O:19]C)=[O:18])=[CH:10][CH:9]=[CH:8][C:7]=2[CH2:6]1)(=O)C>Cl>[NH2:4][CH:5]1[CH2:14][CH2:13][C:12]2[C:11]([O:15][CH2:16][C:17]([OH:19])=[O:18])=[CH:10][CH:9]=[CH:8][C:7]=2[CH2:6]1

Participants

3

Reactant 1

HCID 14014974HCID 14014974, compound

Product 1

HCID 14014982HCID 14014982, compound

Reagents, catalysts & solvents 1

HCID 313Hydrochloric AcidSolvent

Conditions

Temperature
0 °C

Procedure

20 mmol of methyl 6-acetylamino-5,6,7,8-tetrahydro-naphth-1-yl-oxyacetate are refluxed in 300 ml of 2N HCl for 24 hours. The product precipitates on cooling to 0° C.

Workup

  1. customThe product precipitates

Sources & evidence

ORD record
ord-54d3636d8a844748b180691874f8dd6d
Source dataset
uspto-grants-1989_09
Patent number
US04868331

Reaction notes

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