HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Thioglycolate → HCID 19848474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Thioglycolate | HCID 16907 | — |
| Reactant | 2,2-Dimethylaziridine | HCID 227244 | — |
| Product | HCID 19848474 | HCID 19848474 | — |
Reaction Steps
2,2-Dimethylaziridine (35.5 g) was added dropwise with stirring at 100° C. to methyl mercaptoacetate (53 g) during 1.5 hours. After a further 2 hours at 100° C., the mixture was cooled and crystallized from ethyl acetate. Melting point: 151-152° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870063 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-36d5aa992e1f4219be0d63e4519d1ac2 |
| Source note | uspto-grants-1989_09 |