HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propane sultone → HCID 14834685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propane sultone | HCID 14264 | — |
| Reactant | Piperazin-4-ylacetophenone | HCID 97269 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 14834685 | HCID 14834685 | — |
Reaction Steps
A 4.1 g quantity (20 mmols) of 1-(p-acetylphenyl)piperazine is dissolved in 40 ml of acetone, and a solution of 2.44 g (20 mmols) of 1,3-propanesultone in 10 ml of acetone is added dropwise thereto at room temperature with stirring. After reaction at room temperature with stirring overnight, the yellow crystals precipitated are collected by filtration and then recrystallized from water-acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870078 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-3c3d0ec0cca741019105638558cda709 |
| Source note | uspto-grants-1989_09 |