HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoylhydrazine → HCID 53808319, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoylhydrazine | HCID 11955 | — |
| Reactant | 2-Quinolinecarboxaldehyde | HCID 79619 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53808319 | HCID 53808319 | 50% |
Reaction Steps
A mixture of 4.08 gm (0.03 mole) of benzhydrazide, 4.72 gm (0.03 mole) of 2-quinolinecarboxaldehyde and 100 ml of absolute ethanol is refluxed 4 hr. The hot solution is filtered and cooled slowly to room temperature. The mixture is chilled. The crystals which separate are collected, washed with ether and dried to give 4.06 gm (50%) of the title compound having a melting point of 170.7° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04870082 |
| Source dataset | uspto-grants-1989_09 |
| ORD ID | ord-20daf477a49f4711a728d4682696e8e7 |
| Source note | uspto-grants-1989_09 |